Synthesis and Crystal Structure of Potassium Tetranitrato Palladate(II)
K2 [Pd(NO3)4] has been prepared and its crystal structure determined by use of a CAD-4 diffractometer with monochromatic Mo Kα radiation. The space group is P21/c with Z = 4; a= 7.940(2); b = 15.469(4); c = 9.453(2) Å; β = 91.10(3)°. The refinement converged to R = 0.023. The structure contains discrete complexes of [Pd(NO3)4]2− with pseudo symmetry C4. Pd coordinates four oxygen from different unK2[Pd(NO3)4] has been prepared and its crystal structure determined by use of a CAD-4 diffractometer with monochromatic Mo Kα radiation. The space group is P21/c with Z = 4; a= 7.940(2); b = 15.469(4); c = 9.453(2) Å; β = 91.10(3)°. The refinement converged to R = 0.023. The structure contains discrete complexes of [Pd(NO3)4]2− with pseudo-symmetry C4. Pd coordinates four oxygens from different un