Impact of mass transport on meniscus electrochemistry determined by time-resolved operando X-ray photoelectron spectroscopy
Ambient pressure X-ray photoelectron spectroscopy (APXPS) combined with the dip-and-pull method can be used for operando studies of electrochemical systems. A complete coupling between the spectroscopic and the electrochemical measurements is generally challenging due to an inherent difference between the meniscus and the bulk electrolyte - the mass transport. This work investigates meniscus mass
